Sample Reaction System

A two-chamber 5mm glass system for mixing and monitoring a reaction by NMR.

Easy to use-no special equipment is needed. The Inner Chamber, with Teflon Tip, makes a positive seal before mixing.

Basic Operation:
With the central tube (Inner Chamber) pressed against the bottom of the outer tube (the set screw will help maintain the seal), load one component into the chamber.

The Outer Chamber can be loaded, with a syringe, through a side port at the top of the device.

Take initial spectra of the isolated materials.

Eject the system, loosen the set screw, and gently raise the inner tube to a position above the receiver coil. This will begin the mixing of the components.

Lower the device and begin collecting data on the progress of the reaction.

Support data illustrating the Fischer Esterification Reaction is available by clicking